Neue Syntheseverfahren fuer Nitrosoperfluoralkane CnF(2n+1)NO (n = 1, 2, 3, 6)

DOI: 10.1016/0022-1139(95)03237-8

Source and publish data:

Journal of Fluorine Chemistry p. 273 - 274 (1995)

Update date:2022-08-30

Topics:

Authors:

Ludovici, K.

Naumann, D.

Siegemund, G.

Tyrra, W.

Varbelow, H.-G.

Wrubel, H.

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Article abstract of DOI:10.1016/0022-1139(95)03237-8

Perfluoronitrosomethane, CF3NO, may be isolated in ca. 50percent yield of a reaction mixture of i-C3H7ONO2 with ZnBr(CF3)*2CH3CN in the presence of aluminium trichloride.Approximately quantitative yields of CnF(2n+1)NO (n = 1, 2, 3, 6) may be obtained by reacting NOCl with Cd(CnF(2n+1))2*glyme.The preparations are described. - Keywords: Perfluoronitrosoalkanes; Syntheses; F-Alkylcadmium complexes

Full text of DOI:10.1016/0022-1139(95)03237-8

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