Inorganic Chemistry p. 3108 - 3110 (1978)
Update date:2022-08-30
Topics:
Yasumura, Takashi
Lagow, Richard J.
A new synthesis for a number of perfluoroalkyl di-, tri-, and tetrasulfides (CF3SnCF3, C2F5SnCF3, C2F5SnC2F5, n = 2-4) has been developed using a low-temperature glow discharge to dissociate sulfur vapor and generate trifluoromethyl radicals from hexafluoroethane. These compounds were characterized by mass spectra, infrared spectra, and NMR spectra.
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