Fluorination of Trimethylsilyl Phosphites and Their Structural Analogues by Sulphuryl Chloride Fluoride. A Facile Preparation of Phosphorofluoridates and Related Compounds

DOI: 10.1039/c39870000755

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 755 - 756 (1987)

Update date:2022-08-11

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Authors:

Dabkowski, W.

Michalski, J.

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Article abstract of DOI:10.1039/c39870000755

Trimethylsilyl esters of general formula RR'POSiMe3 react in a quantitative and fully chemoselective way with sulphuryl chloride fluoride to give phosphorofluoridates RR'P(O)F of high purity under extremely mild conditions.

Full text of DOI:10.1039/c39870000755

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