Journal of Coordination Chemistry p. 4345 - 4354 (2015)
Update date:2022-08-29
Topics:
Dehghani-Firouzabadi, Ahmad Ali
Kargar, Hadi
Eslaminejad, Safie
Notash, Behrouz
Reactions of 1,2-di(o-aminophenylthio)ethane with 3-ethoxy-2-hydroxybenzaldehyde yield the new hexadentate N2S2O2 donor thioether Schiff base 1,2-bis(2-((2-(thio)phenylimino)methyl)-6-ethoxyphenol)ethane (H2L). Ni(II), Zn(II), Cd(II), and Hg(II) complexes of this ligand were prepared. Of these complexes, [NiL]·2H2O has been structurally characterized by X-ray crystallography. The coordination geometry around Ni(II) was described as octahedral. Zn(II), Cd(II), and Hg(II) complexes and the Schiff base ligand have been characterized by CHN analyses, molar conductivity, UV-vis, FT-IR, 1H, and 13C NMR spectroscopy.
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