Bulletin of the Chemical Society of Japan p. 166 - 169 (1990)
Update date:2022-08-17
Topics:
Hosokawa
Ataka
Murahashi
Alkenes bearing electron-withdrawing substituents are catalytically acetalized with 1,3-propanediol only by the use of PdCl2(MeCN)2 catalyst under O2 atmosphere. When a combination of BiCl3 and LiCl is used as co-catalyst, the acetalization proceeds effectively. These results indicate that a hydroperoxopalladium(II) species is most likely an active catalyst in the present reaction.
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