Tetrahedron Asymmetry p. 655 - 656 (1993)
Update date:2022-08-10
Topics:
Bensch
Mosandl
Fischer
From racemic 4-hydroxypentan-2-one and (S)-tetrahydro-5-oxo-2-furancarboxylic acid chloride the corresponding diastereomeric esters were generated, subsequently separated by liquid chromatography and hydrolyzed to yield pure enantiomers of 4-hydroxypentan-2-one. The X-ray crystal structures of the diastereomeric esters as well as the odour impression of the pure 1,3-ketol enantiomers are reported.
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