Journal of the Chemical Society. Chemical communications p. 167 - 168 (1991)
Update date:2022-08-11
Topics:
Akaji, Kenichi
Tatsumi, Tadashi
Yoshida, Makoto
Kimura, Tooru
Fujiwara, Yoichi
Kiso, Yoshiaki
Methyltrichlorosilane or tetrachlorosilane in trifluoroacetic acid, in the presence of diphenylsulphoxide, is found to cleave various S-protecting groups of cysteine to form cystine directly by the reduction-oxidation reaction; this new disulphide bond forming reaction is successfully applied to the syntheses of oxytocin and human brain natriuretic peptide.
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