Bulletin of the Chemical Society of Japan p. 724 - 726 (1983)
Update date:2022-08-30
Topics:
Ishikawa, Nobuo
Yokozawa, Tsutomu
The preparative method for dimethyl (trifluoromethyl)malonate (4) from the adduct of perfluoro-2-methylpropene with methanol was improved, and several reactions of this base-sensitive substance were investigated.Alkylation of 4 was achieved by using CsF as a condensing agent, and the Michael addition on vinyl ketones proceeded in triethylamine-pyridine medium.
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