Russian Chemical Bulletin p. 756 - 758 (1995)
Update date:2022-08-17
Topics:
Vinogradov, M. G.
Gorshkova, L. S.
Ferapontov, V. A.
Zinenkov, A. V.
A selective method for the preparation of 5-chloropentan-2-one by interaction of 1-methylcyclobutanol with Ca(OCl)2 followed by decomposition of the hypochlorite thus obtained in the presence of FeII salt is proposed.The selectivity of the ketone formation from the alcohol is 98percent, while the conversion of the alcohol is 35-40percent. - Key words: 5-chloropentan-2-one, 1-methylcyclobutanol, 1-methylcyclobutylhypochlorite, free radical decomposition.
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