8
B. L. REID ET AL.
m, 1368 s, 1311 m, 1277 m, 1178 w, 1150 m, 1073 w, 1027 w, 1013 w, 999 w, 928 w, 897 m, 823 w, 780
w, 745 m, 694 m, 668 cm−1 w.
4
.3.2. [Gd(Rb·HOEt)(L)4]2
M.p. 263–264 °C; elemental Anal. Calcd (%) for C180H132Gd Rb O : C, 67.64; H, 4.16; found: C, 67.65; H,
2
2
26
3.51; the elemental analysis deviates somewhat from the theoretical values, possibly due to the presence
of multiple solvates; ATR-IR: v = 3650 w, 3571 w, 3057 w, 3021 w, 1645 m, 1610 w, 1584 s, 1543 s, 1491
m, 1448 m, 1369 s, 1311 m, 1278 m, 1179 w, 1151 m, 1074 w, 1027 w, 1013 w, 999 w, 925 w, 898 m, 823
w, 812 w, 780 w, 747 m, 694 m, 669 cm−1 w.
4
.3.3. [Tb(Na·HOEt)(L)4]2
M.p. 262–263 °C; elemental Anal. Calcd (%) for C180H132Tb Na O : C, 70.31; H, 4.33; found: C, 69.74; H,
2
2
26
4
.33; elemental analysis deviates somewhat from the theoretical values, possibly due to the presence
of multiple solvates; ATR-IR: v = 3644 w, 3557 w, 3058 w, 3032 w, 1645 m, 1584 s, 1543 s, 1491 m, 1448
m, 1369 s, 1311 m, 1278 m, 1179 w, 1150 m, 1073 w, 1027 w, 1013 w, 999 w, 974 w, 923 w, 898 m, 823
w, 780 w, 746 m, 694 m, 669 cm−1 w.
4
.3.4. [Tb(K·HOEt)(L)4]2
M.p. 239–241 °C; elemental Anal. Calcd (%) for C180H132Tb K O ·1.5(H O): C, 68.98; H, 4.34; found: C,
2
2
26
2
6
8.50; H, 3.83; elemental analysis deviates somewhat from the theoretical values, possibly due to the
presence of multiple solvates; ATR-IR: v = 3648 w, 3567 w, 3057 w, 3024 w, 1645 m, 1609 w, 1584 s, 1542
s, 1491 m, 1448 m, 1368 s, 1311 m, 1277 m, 1179 w, 1151 m, 1073 w, 1027 w, 1013 w, 999 w, 975 w, 929
-1
w, 897 m, 823 w, 780 w, 747 m, 694 m, 669 cm w.
4
.3.5. [Tb(Rb·HOEt)(L)4]2
M.p. 263–264 °C; elemental Anal. Calcd (%) for C180H132Tb Rb O ·3(H O): C, 66.44; H, 4.27; found: C,
2
2
26
2
6
6.13; H, 3.35; the elemental analysis deviates somewhat from the theoretical values, possibly due to
the presence of multiple solvates; ATR-IR: v = 3650 w, 3575 w, 3056 w, 3024 w, 1644 m, 1609 w, 1584 s,
544 s, 1491 m, 1447 m, 1369 s, 1311 m, 1276 m, 1179 w, 1153 m, 1073 w, 1027 w, 1013 w, 999 w, 925
1
-1
w, 897 m, 824 w, 780 w, 748 m, 694 m, 669 cm w.
4
.3.6. [Dy(K·HOEt)(L)4]2
M.p. 262–263 °C; elemental Anal. Calcd (%) for C180H132Dy K O : C, 69.42; H, 4.27; found: C, 69.60; H,
2
2
26
3
.78; ATR-IR: v = 3650 w, 3563 w, 3055 w, 3019 w, 2972 w, 1645 m, 1609 w, 1584 m, 1545 s, 1490 m, 1447
m, 1371 s, 1310 m, 1279 m, 1193 w, 1177 w, 1151 m, 1072 w, 1028 w, 1010 w, 975 w, 927 w, 898 m, 824
w, 780 w, 749 m, 694 m, 668 cm−1 w.
4
.3.7. [Dy(Rb·HOEt)(L)4]2
M.p. 267–268 °C; elemental Anal. Calcd (%) for C180H132Dy Rb O ·0.5(H O): C, 67.23; H, 4.17; found: C,
2
2
26
2
6
6.81; H, 3.59; the elemental analysis deviates somewhat from the theoretical values, possibly due to
the presence of multiple solvates; ATR-IR: v = 3653 w, 3571 w, 3057 w, 1645 m, 1611 w, 1584 s, 1545 s,
491 m, 1447 m, 1373 s, 1311 m, 1277 m, 1178 w, 1151 m, 1073 w, 1027 w, 1013 w, 999 w, 976 w, 925
1
−1
w, 898 m, 823 w, 812w, 780 w, 748 m, 694 m, 668 cm w.
4
.3.8. [Ho(K·HOEt)(L)4]2
M.p. 260–261 °C; elemental Anal. Calcd (%) for C180H132Ho K O : C, 69.31; H, 4.27; found: C, 69.11; H,
2
2
26
3
.87; ATR-IR: v = 3567 w, 3059 w, 3019 w, 2968 w, 1668 m, 1644 m, 1611 w, 1584 s, 1546 s, 1490 m, 1447
m, 1389 s, 1371 s, 1310 m, 1279 m, 1195 w, 1180 w, 1179 w, 1151 m, 1074 w, 1024 w, 1012 w, 999 w, 927
w, 898 m, 840 w, 823 w, 778 w, 749 m, 749 w, 694 m, 668 cm− w.
1