Journal of labelled compounds and radiopharmaceuticals p. 465 - 470 (1995)
Update date:2022-08-16
Topics:
Fielder
Rowan
6,6,6-2H3-3Z-Hexenal (3b) has been prepared in 89% yield and in greater than 94% purity by the oxidation of 6,6,63H3-3Z-Hexen-1-of (2b) with the Dess/Martin periodinane (1) in fluorotrichloromethane (freon 11). Use of the freon solvent greatly improved the recovery of this volatile aldehyde. Similarly the oxidation of 3,4-2H2-3Z-hexen-1-of (5) yielded 3,4-2H2-3Z-hexenal (6) in a 92% isolated yield with a purity of greater than 99%. 3,4-2H2-3Z-Hexen-1-of (5) Was prepared in 87% by the catalytic deuterogenation of 3-hexyn-1-of (4) in an improved synthetic procedure,
View More
website:http://www.arromax.com
Contact:+86-0512-62959601 skype:aimmezhang
Address:Suite 401, Bldg A3, 218 Xinghu St.Suzhou Industrial Park 215123, P.R. China
Anhui Jiatiansen Agrochemical Co.,Ltd
Contact:15366811918
Address:chemical industrial park,xiangyu town,dongzhi county,anhui,china
SHANDONG CREDAGRI CHEMICAL CO., LTD.
Contact:+86-531-88872050
Address:ROOM 601A, BUILDING 2, SHUNTAI SQUARE, NO. 2000 SHUNHUA ROAD, HI-TECH DEVELOPMENT ZONE, JINAN, CHINA.
Shanghai PuYi Chem-Tech Co.,Ltd.
Contact:+86-21-57687505-227
Address:3 Floor, Building 11, No 201 MinYi Road, Songjiang District, Shanghai 201612, China
Hubei Onward Bio-Development Co., Ltd.
Contact:+86-718-8417012
Address:No.517,Shizhou Avenue,Enshi City,Hubei Province,China,445002
Doi:10.1016/j.jssc.2012.11.011
(2013)Doi:10.1002/cssc.201802744
(2019)Doi:10.1016/j.dyepig.2017.01.063
(2017)Doi:10.1016/0040-4039(95)01816-Z
(1995)Doi:10.1021/ja01201a008
(1947)Doi:10.1039/c8ta09973a
(2019)
