Magnetic Resonance in Chemistry p. 232 - 235 (1985)
Update date:2022-08-11
Topics:
Srivastava, S.
Cheung, C. K.
Noble, W. J. de
The E- and Z-5-deuterioadamantan-2-ols have been synthesized by an unambiguous route.The 13C NMR spectra show the familiar 1:1:1 splitting of one of the C-5 or C-7 signals, thus allowing a definite assignment of the δ-atoms to be made.This assignment is in accord with the conclusion of Duddeck and Islam.Revised assignments are offered for the reported configurations of the 5-bromo- and -chloro-adamantan-2-ols, and several unusual deuterium isotope shifts are reported.
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