Journal of Organic Chemistry p. 290 - 295 (2015)
Update date:2022-08-04
Topics:
Xia, Xiao-Feng
Gu, Zhen
Liu, Wentao
Wang, Haijun
Xia, Yongmei
Gao, Haiyan
Liu, Xiang
Liang, Yong-Min
A novel and facile oxyazidation of alkenes under metal-free and mild conditions has been reported. A remarkable feature of the developed procedure is consecutive construction of C-O and C-N bonds in one step. The process allows quick and selective assembly of alkyl azide from readily available starting materials, where N-hydroxyphthalimide was used as an oxygen-radical precursor and TMSN3 as the N3 source. A range of aromatic alkenes bearing synthetically useful functional groups was tolerated.
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