Journal of Organometallic Chemistry p. C29 - C32 (1984)
Update date:2022-08-11
Topics:
Lukevics, E.
Dirnens, V. V.
Goldberg, Y. S.
Liepinsh, E. E.
Kalvinsh, I. Ya.
Shimanska, M. V.
Addition of methyl N,N-dichlorocarbamate to trimethylvinylsilane with subsequent reduction with sodium hydrosulphite afforded methyl N-(2-chloro-2-trimethylsilyl)ethylcarbamate.Intramolecular alkylation of the latter in a hexane/solid NaOH two-phase system in the presence of a phase transfer catalyst or under ultrasonic irradiation resulted in 1-carbomethoxy-2-trimethylsilylaziridine.Similarly, starting from trimethylallylsilane the 1-carbethoxy-2-(trimethylsilylmethyl)aziridine was prepared.
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