Tetrahedron Letters p. 9369 - 9372 (1996)
Update date:2022-08-11
Topics:
Gill, G. Bryon
Pattenden, Gerald
Roan, Graeme A.
In a combination of cobalt-mediated cationic and free radical chemistry, treatment of the allyl silane substituted β-hydroxycobaloxime 13 with pTSA led predominantly to the trans-disubstituted cyclopentane 14, which on irradiation with TEMPO produced 15. In a similar manner, the cobaloxine 18 was cyclised to 19 in the presence of pTSA which, on irradiation with a sunlamp then underwent radical mediated cyclisation to the substituted indane 20.
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