An Improved Procedure for the Preparation of Very Pure Ethanol-OD

DOI: 10.1007/BF00809165

Source and publish data:

Monatshefte fur Chemie p. 877 - 878 (1985)

Update date:2022-08-10

Topics:

Authors:

Pesendorfer, Johann

Vierhapper, Friedrich W.

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Article abstract of DOI:10.1007/BF00809165

Changed molar ratio of starting materials and prolonged reaction times in the deuterolysis of tetraethylorthosilicate gave yields of pure (>99.5percent) ethanol-OD (relative to starting D2O) nearly twice of that of a literature procedure. - Keywords: Deuterolysis; Ethanol-OD; Methanol-OD; Tetraethylorthosilicate

Full text of DOI:10.1007/BF00809165

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