Journal of Organic Chemistry p. 966 - 968 (1995)
Update date:2022-08-16
Topics:
Eaton, Philip E.
Li, Jianchang
Upadhyaya, Subhash P.
Details for preparation of 1,4-diiodocubane from cubane-1,4-dicarboxylic acid are given.The diiodide is used to generate cubane-1,4-diyl, a nonisolable intermediate.Additions to the diyl are shown to provide for the ready synthesis in good yield of methylcubane, 1,4-dimethylcubane, cyclopropylcubane, etc.
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