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Cas Database |
| Name |
Pentaerythritol triacrylate |
EINECS | 222-540-8 |
| CAS No. | 3524-68-3 | Density | 1.179 g/cm3 |
| PSA | 99.13000 | LogP | 0.15270 |
| Solubility | insoluble in water | Melting Point |
15℃ |
| Formula | C14H18O7 | Boiling Point | 427.9 ºC at 760 mmHg |
| Molecular Weight | 298.293 | Flash Point | 153.5 °C |
| Transport Information | UN 3265 | Appearance | viscous yellow liquid |
| Safety | 39 | Risk Codes | 36/38-43 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
2-Propenoicacid, 2-(hydroxymethyl)-2-[[(1-oxo-2-propenyl)oxy]methyl]-1,3-propanediyl ester(9CI);Acrylic acid, triester with pentaerythritol (7CI,8CI);Pentaerythritol,triacrylate (8CI);A-TMM 3OHV122;A-TMMA;Agi Syn 2884;Aronix M 30;Aronix M305;Aronix M 306;Gafgard 233;Hipenny;Kayarad PET 30;Light Acrylate PE 3A;Light Ester PE 3A;M 305;NK Ester A-TMN 3LM-N;NK Ester TMM 50T;NewfrontierPET 3;P 300;P 300 (acrylate);PE 3A;PET 30;PETA;PETIA;Pentaerythrityltriacrylate;SR 444;SR 444C;SR 444D;Sartomer 444;Sartomer SR 444;SetaluxUV 2242;Tetramethylolmethane triacrylate;Viscoat 300PETA;2-Propenoic acid,1,1'-[2-(hydroxymethyl)-2-[[(1-oxo-2-propen-1-yl)oxy]methyl]-1,3-propanediyl]ester; |
Article Data | 8 |
Pentaerythritol triacrylate Synthetic route
| Conditions | Yield |
|---|---|
| Stage #1: Pentaerythritol; acrylic acid With IR-120 strong acid type ion exchange resin at 100℃; for 0.5h; Stage #2: In benzene at 100℃; for 3h; Temperature; | 88% |
| Conditions | Yield |
|---|---|
| With triethylamine; trichlorophosphate In (2S)-N-methyl-1-phenylpropan-2-amine hydrate |
- 115-77-5
Pentaerythritol
- 3121-61-7
2-methoxyethyl acrylate
B
- 4986-89-4
pentaerythritol tetraacrylate
C
- 3524-68-3
pentaerythritol triacrylate
| Conditions | Yield |
|---|---|
| With zinc diacetate; oxygen; 4-methoxy-phenol; 1,8-diazabicyclo[5.4.0]undec-7-ene at 105 - 120℃; for 5h; Reagent/catalyst; Inert atmosphere; Overall yield = 48 %; |
- 115-77-5
Pentaerythritol
- 3121-61-7
2-methoxyethyl acrylate
A
- 4986-89-4
pentaerythritol tetraacrylate
B
- 3524-68-3
pentaerythritol triacrylate
| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane; zinc diacetate; oxygen; 4-methoxy-phenol at 105 - 120℃; under 130 - 760 Torr; for 30h; Inert atmosphere; Overall yield = 96 %; | |
| With 1,4-diaza-bicyclo[2.2.2]octane; zinc diacetate; oxygen; 4-methoxy-phenol at 105 - 120℃; under 130 - 760 Torr; for 30h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Overall yield = 88 %; | |
| With 1,4-diaza-bicyclo[2.2.2]octane; zinc diacetate; oxygen; 4-methoxy-phenol at 105 - 120℃; under 130 - 760 Torr; for 30h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Overall yield = 88 %; |
| Conditions | Yield |
|---|---|
| With triphenylphosphine at 90℃; for 8h; | 99.9% |
| Conditions | Yield |
|---|---|
| In toluene for 3h; Diels-Alder Cycloaddition; Inert atmosphere; Schlenk technique; | 97% |
- 3524-68-3
pentaerythritol triacrylate
| Conditions | Yield |
|---|---|
| With acetic acid butyl ester; hydroxyethyl cellulose; dibenzoyl peroxide In water at 80℃; for 8h; Product distribution; Further Variations:; Reagents; | 96.6% |
| Conditions | Yield |
|---|---|
| With 4-methoxy-phenol; triphenylphosphine at 95℃; for 14h; | 94.58% |
| Conditions | Yield |
|---|---|
| With 4-methoxy-phenol; triphenylphosphine at 90℃; for 8h; | 91.2% |
| Conditions | Yield |
|---|---|
| With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 20h; | 85% |
Pentaerythritol triacrylate Chemical Properties
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IUPAC Name: [2-(Hydroxymethyl)-3-prop-2-enoyloxy-2-(prop-2-enoyloxymethyl)propyl] prop-2-enoate
Empirical Formula: C14H18O7
Molecular Weight: 298.2885
EINECS: 222-540-8
Product Categories: Functional Monomer; RAW material for negative PR
storage temp.: 2-8 °C
Sensitive: Hygroscopic
Stability: Stable at room temperature, but potentially explosive at elevated temperatures. Combustible, but may explode if involved in a fire.
Index of Refraction: 1.488
Molar Refractivity: 72.91 cm3
Molar Volume: 252.9 cm3
Surface Tension: 41.5 dyne/cm
Density: 1.179 g/cm3
Flash Point: 153.5 °C
Enthalpy of Vaporization: 78.86 kJ/mol
Boiling Point: 427.9 °C at 760 mmHg
Vapour Pressure: 4.08E-09 mmHg at 25 °C
Appearance: Thick clear yellow liquid.
Classification Code of Pentaerythritol triacrylate (CAS NO.3524-68-3): Mutation data; Reproductive Effect; Skin / Eye Irritant; Tumor data
Pentaerythritol triacrylate Toxicity Data With Reference
| Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
|---|---|---|---|---|---|
| rabbit | LD50 | skin | 4mL/kg (4mL/kg) | Toxicology and Applied Pharmacology. Vol. 28, Pg. 313, 1974. | |
| rat | LD50 | intraperitoneal | 25mg/kg (25mg/kg) | BEHAVIORAL: ATAXIA GASTROINTESTINAL: OTHER CHANGES SKIN AND APPENDAGES (SKIN): HAIR: OTHER | National Technical Information Service. Vol. OTS0555706, |
| rat | LD50 | oral | 1830mg/kg (1830mg/kg) | GASTROINTESTINAL: ULCERATION OR BLEEDING FROM SMALL INTESTINE GASTROINTESTINAL: ULCERATION OR BLEEDING FROM LARGE INTESTINE GASTROINTESTINAL: OTHER CHANGES | National Technical Information Service. Vol. OTS0555713, |
Pentaerythritol triacrylate Consensus Reports
Reported in EPA TSCA Inventory.
Pentaerythritol triacrylate Safety Profile
Moderately toxic by ingestion and skin contact. Skin and severe eye irritant. Questionable carcinogen with experimental tumorigenic data. Used for radiation-cured adhesives, coatings, inks, textiles, photo resists, and coatings. When heated to decomposition it emits acrid smoke and irritating fumes.
Hazard Codes: 
Xi
Risk Statements: 36/38-43
R36/38:Irritating to eyes and skin.
R43:May cause sensitization by skin contact.
Safety Statements: 39
S39:Wear eye / face protection.
RIDADR: UN3265
WGK Germany: 1
RTECS: UD3370000
HazardClass: 8
PackingGroup: III
Pentaerythritol triacrylate Specification
Pentaerythritol triacrylate (CAS NO.3524-68-3), its Synonyms are Pentaerythrityl triacrylate ; Acrylic acid, triester with pentaerythritol ; Aronix M 305 ; Gafgard 233 ; Kayarad PET 30 ; Light Acrylate PE 3A ; NK Ester A-TMM 3 ; NK Ester A-TMM 3L ; NK Ester TMM 50T ; 2-(Hydroxymethyl)-2-(((1-oxoallyl)oxy)methyl)-1,3-propanediyl diacrylate ; 2-Propenoic acid, 1,1'-(2-(hydroxymethyl)-2-(((1-oxo-2-propen-1-yl)oxy)methyl)-1,3-propanediyl) ester ; 2-Propenoic acid, 2-(hydroxymethyl)-2-(((1-oxo-2-propenyl)oxy)methyl)-1,3-propanediyl ester .
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