4-METHOXY-2'-METHYLBENZOPHENONE

Base Information

• Chemical Name: 4-METHOXY-2'-METHYLBENZOPHENONE
• CAS No.: 41204-59-5
• Molecular Formula: C15H14O2
• Molecular Weight: 226.275
• Hs Code.: 2914509090
• Mol file: 41204-59-5.mol

Synonyms:4-Methoxyphenyl 2-methylphenyl ketone;4-METHOXY-2'-METHYLBENZOPHENONE;2-methyl-4'-methoxybenzophenone;

Chemical Property of 4-METHOXY-2'-METHYLBENZOPHENONE

Chemical Property:

• Vapor Pressure: 0.000108mmHg at 25°C
• Boiling Point: 336.9oC at 760 mmHg
• Flash Point: 144.3oC
• PSA: 26.30000
• Density: 1.088g/cm3
• LogP: 3.23460

Purity/Quality:

97% ^*data from raw suppliers

2-Methyl-4''-methoxybenzophenone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-METHOXY-2'-METHYLBENZOPHENONE

There total 42 articles about 4-METHOXY-2'-METHYLBENZOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-methoxy-benzaldehyde (123-11-5) + potassium o-tolyltrifluoroborate → (4-methoxyphenyl)(2-methylphenyl)methanone (41204-59-5)

Guidance literature:

With potassium carbonate; tri tert-butylphosphoniumtetrafluoroborate; bis(ethylene)rhodium(I) chloride dimer; In 1,4-dioxane; acetone; at 80 ℃;

DOI:10.1021/jo801460w

Reference yield: 96.0%

o-tolyl magnesium chloride (33872-80-9) + 4-methoxy-benzoyl chloride (100-07-2) → (4-methoxyphenyl)(2-methylphenyl)methanone (41204-59-5)

Guidance literature:

o-tolyl magnesium chloride; With zinc(II) chloride; In 1-methyl-pyrrolidin-2-one; diethyl ether; at 60 ℃; for 0.333333h;

4-methoxy-benzoyl chloride; ((t-Bu)2POH)2PdCl₂; In 1-methyl-pyrrolidin-2-one; at 25 ℃; for 0.5h; Further stages.;

DOI:10.1021/jo801445y

Reference yield: 92.0%

carbon monoxide (201230-82-2) + para-iodoanisole (696-62-8) + 2-Methylphenylboronic acid (16419-60-6) → (4-methoxyphenyl)(2-methylphenyl)methanone (41204-59-5)

Guidance literature:

With potassium acetate; sodium hydrogencarbonate; iron(II) chloride; at 100 ℃; for 23h; under 760.051 Torr; Schlenk technique;

DOI:10.1039/c4cc00688g

upstream raw materials:

ortho-methylbenzoic acid

methoxybenzene

ortho-toluoyl chloride

(9-anthracenyl)-(2-methylphenyl)-methanone

Downstream raw materials:

(4-Methoxy-3-nitro-phenyl)-o-tolyl-methanone

4-hydroxyphenyl 2-methylphenyl ketone

C₁₈H₁₈O₂

C₁₈H₂₀O₂

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