1,3-Dichloro-2,2-dimethoxypropane

Base Information

• Chemical Name: 1,3-Dichloro-2,2-dimethoxypropane
• CAS No.: 6626-57-9
• Molecular Formula: C5H10Cl2O2
• Molecular Weight: 173.039
• Hs Code.: 2911000000
• Mol file: 6626-57-9.mol

Synonyms:2-Propanone,1,3-dichloro-, dimethyl acetal (8CI);1,3-Dichloro-2,2-dimethoxypropane;1,3-Dichloro-2-propanone dimethyl acetal;1,3-Dichloroacetone dimethyl acetal;1,3-Dichloroacetone dimethyl ketal;NSC 58238;

Chemical Property of 1,3-Dichloro-2,2-dimethoxypropane

Chemical Property:

• Vapor Pressure: 0.629mmHg at 25°C
• Melting Point: 81.5 °C
• Refractive Index: 1.436
• Boiling Point: 194 °C at 760 mmHg
• Flash Point: 69.8 °C
• PSA: 18.46000
• Density: 1.18 g/cm³
• LogP: 1.45310
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

1,3-Dichloro-2,2-dimethoxypropane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Dichloro-2,2-dimethoxypropane

There total 6 articles about 1,3-Dichloro-2,2-dimethoxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1,3-Dichloroacetone (534-07-6) + trimethyl orthoformate (149-73-5) → 1,3-dichloroacetone dimethyl acetal (6626-57-9)

Guidance literature:

With Amberlyst 15; In dichloromethane;

DOI:10.1016/S0040-4020(01)88873-6

Reference yield: 81.2%

methanol (67-56-1) + acetone (67-64-1) → 1,3-dichloroacetone dimethyl acetal (6626-57-9)

Guidance literature:

With chlorine; at 20 - 35 ℃; for 0.5h;

Reference yield:

methanol (67-56-1) + 1,3-Dichloroacetone (534-07-6) → 1,3-dichloroacetone dimethyl acetal (6626-57-9)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

methanol

1,3-Dichloroacetone

trimethyl orthoformate

acetone

Downstream raw materials:

1,3-Dichloroacetone

1-benzyl-3,3-dimethoxyazetidine

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