N-[(2-METHOXYPHENYL)METHYLENE]-N-METHYLAMINE

Base Information

• Chemical Name: N-[(2-METHOXYPHENYL)METHYLENE]-N-METHYLAMINE
• CAS No.: 1125-90-2
• Molecular Formula: C9H11 N O
• Molecular Weight: 149.192
• Hs Code.: 2925290090
• Mol file: 1125-90-2.mol

Synonyms:Benzaldehyde,o-methoxy-, N-methyloxime (3CI); Methylamine, N-(o-methoxybenzylidene)-(6CI,7CI,8CI); 2-Methoxybenzaldehyde N-methylimine;N-(2-Methoxybenzylidene)methylamine

Chemical Property of N-[(2-METHOXYPHENYL)METHYLENE]-N-METHYLAMINE

Chemical Property:

• Vapor Pressure: 0.0516mmHg at 25°C
• Boiling Point: 242.9°Cat760mmHg
• Flash Point: 84.5°C
• PSA: 21.59000
• Density: 0.94g/cm³
• LogP: 1.74390

Purity/Quality:

98%,99%, ^*data from raw suppliers

[(2-Methoxyphenyl)methylidene](methyl)amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-[(2-METHOXYPHENYL)METHYLENE]-N-METHYLAMINE

There total 5 articles about N-[(2-METHOXYPHENYL)METHYLENE]-N-METHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ortho-anisaldehyde (135-02-4) + methylamine (74-89-5) → 1-(2-methoxyphenyl)-N-methylmethanimine (1125-90-2)

Guidance literature:

In ethanol; at 0 - 40 ℃;

DOI:10.1016/j.bmc.2006.09.026

Reference yield: 99.0%

methylammonium N-methylcarbamate (65398-48-3) + ortho-anisaldehyde (135-02-4) → 1-(2-methoxyphenyl)-N-methylmethanimine (1125-90-2)

Guidance literature:

In neat (no solvent); at 25 ℃; for 3h; Inert atmosphere; Green chemistry;

DOI:10.1039/d0ra07814j

Reference yield: 87.0%

methylamine hydrochloride (593-51-1) + ortho-anisaldehyde (135-02-4) → 1-(2-methoxyphenyl)-N-methylmethanimine (1125-90-2)

Guidance literature:

With 1,1'-(1,4-butanediyl)bis(imidazole); In neat (no solvent); at 20 ℃; for 10h; Milling;

DOI:10.1071/CH18408

upstream raw materials:

ortho-anisaldehyde

methylamine

(Z)-C-(2-methoxyphenyl)-N-methyl-nitrone

methylamine hydrochloride

Downstream raw materials:

[1-(2-methoxy-phenyl)-propyl]-methyl-amine

{2-Methoxy-1-(2-methoxy-phenyl)-3-[1-trimethylsilanyl-meth-(E)-ylidene]-hex-5-enyl}-methyl-amine

4-[(2-Methoxy-phenyl)-methylamino-methyl]-5-methyl-2-phenyl-2,4-dihydro-pyrazol-3-one

o-methoxybezylidenedimethylimmonium iodide

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