1-Cyclohexene-1-carboxaldehyde, 2-[(trimethylsilyl)oxy]-

Base Information

Chemical Name:1-Cyclohexene-1-carboxaldehyde, 2-[(trimethylsilyl)oxy]-
CAS No.:62269-45-8
Molecular Formula:C10H18O2Si
Molecular Weight:198.33400
Hs Code.:

Synonyms:1-Formyl-2-trimethylsiloxycyclohexenon;1-Cyclohexene-1-carboxaldehyde,2-[(trimethylsilyl)oxy];

Suppliers and Price of 1-Cyclohexene-1-carboxaldehyde, 2-[(trimethylsilyl)oxy]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Cyclohexene-1-carboxaldehyde, 2-[(trimethylsilyl)oxy]-

Chemical Property:

Boiling Point:221.5±40.0 °C(Predicted)
PSA：26.30000
Density:0.95±0.1 g/cm3(Predicted)
LogP:2.86490

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Cyclohexene-1-carboxaldehyde, 2-[(trimethylsilyl)oxy]-

There total 3 articles about 1-Cyclohexene-1-carboxaldehyde, 2-[(trimethylsilyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 62269-45-8
1-Formyl-2-trimethylsiloxycyclohexenon

Guidance literature:: Multi-step reaction with 2 steps

1: 22.2 g / sodium hydride, ethanol / diethyl ether / 2 h

2: triethylamine / hexane

With ethanol; sodium hydride; triethylamine; In diethyl ether; hexane;
DOI:10.1021/ja00530a038

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 39695-64-2
2-(hydroxymethylene)cyclohexanone

: 62269-45-8
1-Formyl-2-trimethylsiloxycyclohexenon

: 74590-75-3
6-<(trimethylsiloxy)methylene>cyclohexen-2-one

Guidance literature:: With triethylamine; In hexane; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00530a038