Benzenemethanamine, N-[(4-methoxyphenyl)methylene]-

Base Information

• Chemical Name: Benzenemethanamine, N-[(4-methoxyphenyl)methylene]-
• CAS No.: 622-72-0
• Molecular Formula: C15H15NO
• Molecular Weight: 225.29
• Mol file: 622-72-0.mol

Synonyms:N-benzyl-p-methoxyphenylimine;UPCMLD00WMAL2-248;N-benzyl-(4-methoxyphenyl)methanimine;p-methoxybenzylidene-benzyl-amine;N-(4-methoxybenzylidene)benzylamine;N-(4-methoxylbenzylidene)benzylamine;N-(4-methoxybenzylidene)-1-phenylmethanamine;N-[(4-methoxyphenyl)methylidene]aniline;Benzenemethanamine,N-[(4-methoxyphenyl)methylene];

Chemical Property of Benzenemethanamine, N-[(4-methoxyphenyl)methylene]-

Chemical Property:

• Melting Point: 42 °C
• Boiling Point: 216 °C(Press: 12 Torr)
• PSA: 21.59000
• Density: 0.99±0.1 g/cm3(Predicted)
• LogP: 3.31430

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenemethanamine, N-[(4-methoxyphenyl)methylene]-

There total 32 articles about Benzenemethanamine, N-[(4-methoxyphenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-methoxy-benzaldehyde (123-11-5) + benzylamine (100-46-9) → N-(4-methoxylbenzylidene)benzylamine (622-72-0)

Guidance literature:

In chloroform; at 20 ℃; for 1h;

DOI:10.1039/c4cc04668d

Reference yield: 97.0%

4-Methoxybenzyl alcohol (105-13-5) + benzylamine (100-46-9) → N-(4-methoxylbenzylidene)benzylamine (622-72-0)

Guidance literature:

With C₃₀H₂₄AgBr₄N₈⁽¹⁺⁾*AgBr₂^(1-); N-benzyl-trimethylammonium hydroxide; In toluene; at 20 ℃; for 12h; Molecular sieve; Schlenk technique;

DOI:10.1021/ol501353q

Reference yield: 96.0%

(benzylimino)triphenylphosphorane (52826-45-6) + 4-Methoxybenzyl alcohol (105-13-5) → N-(4-methoxylbenzylidene)benzylamine (622-72-0)

Guidance literature:

With C₃₇H₃₆Cl₂NPRuS₂; triphenylphosphine; potassium hydroxide; In toluene; at 135 ℃; for 18h; Inert atmosphere;

DOI:10.1039/c8dt04725a

upstream raw materials:

ethanol

N-(4-methoxybenzyl)benzaldimine

sodium ethanolate

ethyl [2]alcohol

Downstream raw materials:

tert-Butyl N-benzyl-N-carbamate

Benzyl N-benzyl-N-carbamate

N,N-dibenzyl-1,2-bis(4-methoxyphenyl)ethane-1,2-diamine

1,3-Dibenzyl-4,5-bis-(4-methoxy-phenyl)-2-methyl-imidazolidine