α-acetophenonesulfonic acid sodiuM salt

Base Information

• Chemical Name: α-acetophenonesulfonic acid sodiuM salt
• CAS No.: 63738-92-1
• Molecular Formula: C8H8O4S.Na
• Molecular Weight: 222.197
• Mol file: 63738-92-1.mol

Synonyms:A-ACETOPHENONESULFONIC ACID SODIUM SALT;sodium 2-oxo-2-phenylethanesulfonate;acetophenonesulfonic acid sodium salt;2-Oxo-2-phenyl-aethansulfonsaeure, Natrium-Salz;2-oxo-2-phenyl-ethanesulfonic acid , sodium-salt;Na-salz der Acetophenon-ω-sulfonsaeure;

Chemical Property of α-acetophenonesulfonic acid sodiuM salt

Chemical Property:

• PSA: 82.65000
• LogP: 1.49530
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Sodium2-oxo-2-phenylethanesulfonate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of α-acetophenonesulfonic acid sodiuM salt

There total 4 articles about α-acetophenonesulfonic acid sodiuM salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-bromoacetone (598-31-2) + sodium sulfite (7757-83-7) → α-acetophenonesulfonic acid sodium salt (63738-92-1)

Guidance literature:

In not given;

DOI:10.1039/JR9340001861

Reference yield: 70.0%

acetophenone (98-86-2) → α-acetophenonesulfonic acid sodium salt (63738-92-1)

Guidance literature:

With sodium hydroxide; sulfur trioxide; In 1,2-dichloro-ethane; for 2h; <35 deg C;

Reference yield: 66.0%

1-chloroacetophenone (532-27-4,108321-66-0,164322-25-2) → α-acetophenonesulfonic acid sodium salt (63738-92-1)

Guidance literature:

With sodium sulfite; In ethanol; water; for 20h; Heating;

DOI:10.1016/S0040-4020(99)00443-3

upstream raw materials:

acetophenone

1-chloroacetophenone

α-bromoacetophenone

1-bromoacetone

Downstream raw materials:

2-chlorosulfonylacetophenone-ω-sulfonyl chloride

(Z)-2-chloro-2-phenyl-ethenesulfonic acid amide

benzoic acid

2-phenylethynesulfonamide