p-Tetrahydropyranyloxystyrene

Base Information

• Chemical Name: p-Tetrahydropyranyloxystyrene
• CAS No.: 65409-15-6
• Molecular Formula: C13H16O2
• Molecular Weight: 204.269
• DSSTox Substance ID: DTXSID50433127
• Nikkaji Number: J767.075C

Synonyms:p-tetrahydropyranyloxystyrene;65409-15-6;SCHEMBL412542;4-tetrahydropyran-2-yloxystyrene;DTXSID50433127;4-(2-tetrahydropyranyloxy)styrene;OODGPKJPJBOZQL-UHFFFAOYSA-N;2-(4-Vinylphenoxy)tetrahydro-2H-pyran

Chemical Property of p-Tetrahydropyranyloxystyrene

Chemical Property:

• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 204.115029749
• Heavy Atom Count: 15
• Complexity: 195

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CC1=CC=C(C=C1)OC2CCCCO2

Technology Process of p-Tetrahydropyranyloxystyrene

There total 6 articles about p-Tetrahydropyranyloxystyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-(tetrahydropyran-2-yloxy)benzaldehyde (74189-56-3) + diazomethyl-trimethyl-silane (18107-18-1) → 1-(tetrahydropyran-2-yloxy)-4-vinylbenzene (65409-15-6)

Guidance literature:

With Wilkinson's catalyst; triphenylphosphine; isopropyl alcohol; In tetrahydrofuran; at 25 ℃; for 1h;

DOI:10.1021/ja038112o

Reference yield: 81.0%

Methyltriphenylphosphonium bromide (1779-49-3) + 4-(tetrahydropyran-2-yloxy)benzaldehyde (74189-56-3) → 1-(tetrahydropyran-2-yloxy)-4-vinylbenzene (65409-15-6)

Guidance literature:

Methyltriphenylphosphonium bromide; With sodium hexamethyldisilazane; In tetrahydrofuran; at 25 ℃; for 1h;

4-(tetrahydropyran-2-yloxy)benzaldehyde; In tetrahydrofuran; at 25 ℃; for 1h;

DOI:10.1021/ja038112o

Reference yield:

Vinyl bromide (593-60-2,25951-54-6) + dichloro-[1,2-bis(diphenylphosphino)ethane] nickel + 4-(tetrahydropyran-2'-yloxy)-1-bromobenzene (36603-49-3) + ethylene dibromide (106-93-4) → 1-(tetrahydropyran-2-yloxy)-4-vinylbenzene (65409-15-6)

Guidance literature:

With iodine; magnesium; In tetrahydrofuran; water;

upstream raw materials:

3,4-dihydro-2H-pyran

4-Vinylphenol

4-(tetrahydropyran-2-yloxy)benzaldehyde

diazomethyl-trimethyl-silane

Downstream raw materials:

(E)-(2-nitro-5-(4-((tetrahydro-2H-pyran-2-l)oxy)styryl)phenyl)methanol

(E)-2-nitro-5-(4-((tetrahydro-2H-pyran-2-yl)oxy)styryl)benzyl 4-(4-(bis(2-chloroethyl)amino)phenyl)butanoate

(E)-5-(4-hydroxystyryl)-2-nitrobenzyl 4-(4-(bis(2-chloroethyl)amino)phenyl)butanoate

(E)-2-nitro-5-(4-(prop-2-yn-1-yloxy)styryl)benzyl 4-(4-(bis(2-chloroethyl)amino)phenyl)butanoate

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