2H-1,4-Benzoxazine, 3,4-dihydro-4-methyl-

Base Information

Chemical Name:2H-1,4-Benzoxazine, 3,4-dihydro-4-methyl-
CAS No.:77901-22-5
Molecular Formula:C9H11NO
Molecular Weight:149.192
Hs Code.:2934999090
DSSTox Substance ID:DTXSID70395970
Nikkaji Number:J1.091.487F
Mol file:77901-22-5.mol

Synonyms:77901-22-5;2H-1,4-Benzoxazine, 3,4-dihydro-4-methyl-;4-methyl-2,3-dihydro-1,4-benzoxazine;4-methyl-3,4-dihydro-2h-1,4-benzoxazine;4-methyl-3,4-dihydro-2H-benzo[b][1,4]oxazine;4-Methyl-3,4-dihydro-2H-benzo[1,4]oxazine;SCHEMBL519320;DTXSID70395970;YJRQBOOMJGYUPI-UHFFFAOYSA-N;CDA90122;MFCD01651884;AKOS016360132;AS-8329;CS-0312948;W18821

Suppliers and Price of 2H-1,4-Benzoxazine, 3,4-dihydro-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
4-Methyl-3,4-dihydro-2H-1,4-benzoxazine
1 g
$ 373.00

Matrix Scientific
4-Methyl-3,4-dihydro-2H-benzo[1,4]oxazine 95%+
1g
$ 357.00

Advanced Chemicals Intermediatesced Chemicals Intermediates
4-Methyl-3,4-dihydro-2H-benzo[1,4]oxazine 95%+
1g
$ 174.00

Advanced Chemicals Intermediatesced Chemicals Intermediates
4-Methyl-3,4-dihydro-2H-benzo[1,4]oxazine 95%+
10g
$ 1080.25

Acints
4-Methyl-3,4-dihydro-2H-benzo[1,4]oxazine 95%+
10g
$ 1080.25

Acints
4-Methyl-3,4-dihydro-2H-benzo[1,4]oxazine 95%+
5g
$ 609.00

Acints
4-Methyl-3,4-dihydro-2H-benzo[1,4]oxazine 95%+
1g
$ 174.00

Total 5 raw suppliers

Chemical Property of 2H-1,4-Benzoxazine, 3,4-dihydro-4-methyl-

Chemical Property:

PSA：12.47000
LogP:1.58020
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:149.084063974
Heavy Atom Count:11
Complexity:138

Purity/Quality:

99% ^*data from raw suppliers

4-Methyl-3,4-dihydro-2H-1,4-benzoxazine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCOC2=CC=CC=C21

Technology Process of 2H-1,4-Benzoxazine, 3,4-dihydro-4-methyl-

There total 23 articles about 2H-1,4-Benzoxazine, 3,4-dihydro-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 21744-84-3
4-methyl-4H-benzo[1,4]oxazin-3-one

: 77901-22-5
4-methyl-3,4-dihydro-2H-benzo[b][1,4]oxazine

Guidance literature:: With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 65 ℃; for 1h;
DOI:10.1016/S0040-4039(99)00556-0

Reference yield: 92.0%

: 124-38-9,18923-20-1
carbon dioxide

: 5735-53-5
1,4-benzoxazine

: 77901-22-5
4-methyl-3,4-dihydro-2H-benzo[b][1,4]oxazine

Guidance literature:: With cyclopentadienyl iron(II) dicarbonyl dimer; phenylsilane; triphenylphosphine; In acetonitrile; at 100 ℃; for 36h; under 760.051 Torr; Schlenk technique; Sealed tube;
DOI:10.1002/adsc.201900906