Stannane, 1,4-butanediylbis[trichloro-

Base Information

Chemical Name:Stannane, 1,4-butanediylbis[trichloro-
CAS No.:83563-65-9
Molecular Formula:C4H8Cl6Sn2
Molecular Weight:506.246
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, 1,4-butanediylbis[trichloro-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Stannane, 1,4-butanediylbis[trichloro-

There total 1 articles about Stannane, 1,4-butanediylbis[trichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 5274-40-8
1,4-bis(triphenylstannyl)butane

: 7646-78-8
tin(IV) chloride

: 83563-65-9
α,ω-bis-(trichlorostannyl)butane

: 1124-19-2
phenyltin trichloride

Guidance literature:: In neat (no solvent); heating for 3 h at 120-130°C; the mixt. was distd. in vac.;
DOI:10.1021/om010202j

Reference yield: 83.0%

: 83563-65-9
α,ω-bis-(trichlorostannyl)butane

: 1100-88-5
benzyltriphenylphosphonium chloride

: 2[C₆H₅CH₂P(C₆H₅)3]⁽¹⁺⁾*[Cl₄Sn(CH₂)4SnCl₄]^(2-)=[C₆H₅CH₂P(C₆H₅)3]2[Cl₄Sn(CH₂)4SnCl₄]

Guidance literature:: In chloroform; (Ar); dropwise addn. of soln. of (PhCH2PPh3)Cl (1 equiv.) in CHCl3 in magnetically stirred soln. of Cl3Sn(CH2)4SnCl3 (2 equiv.) in CHCl3; stirring overnight; filtration, washing twice with CHCl3, recrystn. from CH2Cl2; elem. anal.;
DOI:10.1021/om010246s

Reference yield: 64.0%

: 83563-65-9
α,ω-bis-(trichlorostannyl)butane

: 930-69-8
sodium thiophenolate

: 1,4-bis[tris(thiophenolato)stannyl]butane

Guidance literature:: In methanol; byproducts: NaCl; under Ar or N2; soln. of Sn compd. in dry MeOH added slowly to soln. of NaSPh at 0°C; stirred for 24 h; filtered; washed with MeOH and hexane; dried in vac.; crystd. from CH2Cl2-hexane over 2 d;
DOI:10.1002/zaac.200800263