3-BroMo-2-Methoxyphenol

Base Information

• Chemical Name: 3-BroMo-2-Methoxyphenol
• CAS No.: 88275-88-1
• Molecular Formula: C7H7BrO2
• Molecular Weight: 203.035
• Hs Code.: 2909500000
• Mol file: 88275-88-1.mol

Synonyms:Phenol,3-bromo-2-methoxy;3-Bromo-2-methoxy-phenol;

Chemical Property of 3-BroMo-2-Methoxyphenol

Chemical Property:

• Boiling Point: 252.8±20.0 °C(Predicted)
• PKA: 9.01±0.10(Predicted)
• PSA: 29.46000
• Density: 1.585±0.06 g/cm3(Predicted)
• LogP: 2.16330

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-2-methoxyphenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BroMo-2-Methoxyphenol

There total 12 articles about 3-BroMo-2-Methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3-bromo-2-methyloxybenzaldehyde (88275-87-0) → 3-bromo-2-methoxyphenol (88275-88-1)

Guidance literature:

3-bromo-2-methyloxybenzaldehyde; With potassium dihydrogenphosphate; dihydrogen peroxide; trifluoroacetic anhydride; In dichloromethane; water; at 0 ℃;

With hydrogenchloride; In methanol; water; at 20 ℃; for 0.75h;

DOI:10.1055/s-0037-1609717

Reference yield: 83.0%

C8H7BrO3 → 3-bromo-2-methoxyphenol (88275-88-1)

Guidance literature:

With methanol; triethylamine; at 20 ℃; for 12h;

DOI:10.1021/acs.orglett.1c03998

Reference yield:

sodium carbonate (497-19-8) + 3-bromo-2-methyloxybenzaldehyde (88275-87-0) → 3-bromo-2-methoxyphenol (88275-88-1)

Guidance literature:

With trifluoroacetyl peroxide; sodium; In diethyl ether; dichloromethane;

upstream raw materials:

3-bromo-2-methyloxybenzaldehyde

2-bromo-6-(2-propenyl)phenol

(E)-3-Bromo-2-methoxy-1-prop-1-enylbenzene

3-Brom-2-methoxy-1-(2-propenyl)benzol

Downstream raw materials:

2-methoxy-3-tetrahydropyranyloxy-1-bromobenzene

(2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanone

2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

(1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

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