Benzene, 1-methoxy-4-(1-methoxypropyl)-

Base Information

Chemical Name:Benzene, 1-methoxy-4-(1-methoxypropyl)-
CAS No.:88932-42-7
Molecular Formula:C11H16O2
Molecular Weight:180.247
Hs Code.:
DSSTox Substance ID:DTXSID80404789
Nikkaji Number:J859.761H

Synonyms:Benzene, 1-methoxy-4-(1-methoxypropyl)-;88932-42-7;SCHEMBL17666418;DTXSID80404789

Suppliers and Price of Benzene, 1-methoxy-4-(1-methoxypropyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzene, 1-methoxy-4-(1-methoxypropyl)-

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:180.115029749
Heavy Atom Count:13
Complexity:128

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(C1=CC=C(C=C1)OC)OC

Technology Process of Benzene, 1-methoxy-4-(1-methoxypropyl)-

There total 3 articles about Benzene, 1-methoxy-4-(1-methoxypropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5349-60-0
1-(4-methoxyphenyl)-1-propanol

: 74-88-4
methyl iodide

: 88932-42-7
4-methoxy-α-ethylbenzyl methyl ether

Guidance literature:: 1-(4-methoxyphenyl)-1-propanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 1h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1039/c3ob27128e

Reference yield:

: 67-56-1
methanol

: 4180-23-8,25086-72-0,63589-56-0
E-1-(4'-methoxyphenyl)prop-1-ene

: 88932-42-7
4-methoxy-α-ethylbenzyl methyl ether

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate; Yield given. Multistep reaction; 1) CH₃OH, 30 min, 2) 3 h;
DOI:10.1021/jo00181a021

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 88932-42-7
4-methoxy-α-ethylbenzyl methyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) isopropylate; (R)-1,1'-Bi-2-naphthol / tetrahydrofuran; toluene / 0.5 h / 20 °C

1.2: 5 h / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

2.2: 8 h / 20 °C

With titanium(IV) isopropylate; (R)-1,1'-Bi-2-naphthol; sodium hydride; In tetrahydrofuran; toluene; mineral oil;
DOI:10.1016/j.tetlet.2013.12.083