alpha-(Dimethoxyphosphinyl)-4-methoxybenzenemethanol

Base Information

Chemical Name:alpha-(Dimethoxyphosphinyl)-4-methoxybenzenemethanol
CAS No.:6329-54-0
Molecular Formula:C₁₀H₁₅O₅P
Molecular Weight:246.2
Hs Code.:
NSC Number:43462
Nikkaji Number:J2.648.473A

Synonyms:NSC43462;NSC-43462

Suppliers and Price of alpha-(Dimethoxyphosphinyl)-4-methoxybenzenemethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of alpha-(Dimethoxyphosphinyl)-4-methoxybenzenemethanol

Chemical Property:

Vapor Pressure:1.75E-06mmHg at 25°C
Boiling Point:380.9°C at 760 mmHg
Flash Point:184.2°C
Density:1.244g/cm³
XLogP3:0.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:246.06571057
Heavy Atom Count:16
Complexity:242

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C(O)P(=O)(OC)OC

Technology Process of alpha-(Dimethoxyphosphinyl)-4-methoxybenzenemethanol

There total 7 articles about alpha-(Dimethoxyphosphinyl)-4-methoxybenzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 96-36-6,868-85-9
methyl phosphite

: 123-11-5
4-methoxy-benzaldehyde

: 79296-58-5,6329-54-0
[hydroxy-(4-methoxy-phenyl)-methyl]-phosphonic acid dimethyl ester

Guidance literature:: With triethylamine; magnesium chloride; at 50 ℃; for 2h;
DOI:10.1002/cjoc.201100199

Reference yield: 95.0%

: 123-11-5
4-methoxy-benzaldehyde

: 868-85-9
Dimethyl phosphite

: 79296-58-5,6329-54-0
[hydroxy-(4-methoxy-phenyl)-methyl]-phosphonic acid dimethyl ester

Guidance literature:: 4-methoxy-benzaldehyde; With phosphotungstic acid supported on silica-coated magnetic Fe₃O₄ nanoparticle; In neat (no solvent); at 20 ℃; for 0.25h; Green chemistry;

Dimethyl phosphite; In neat (no solvent); at 20 ℃; for 6h; Green chemistry;
DOI:10.1002/cplu.201402191

Reference yield: 93.0%

: 123-11-5
4-methoxy-benzaldehyde

: 121-45-9
phosphorous acid trimethyl ester

: 79296-58-5,6329-54-0
[hydroxy-(4-methoxy-phenyl)-methyl]-phosphonic acid dimethyl ester

Guidance literature:: With chloro-trimethyl-silane; lithium perchlorate; In diethyl ether; at 20 ℃; for 0.0833333h;
DOI:10.1080/10426500307904