3-Pyridinecarboxylicacid,trimethylsilylester(9CI)

Base Information

• Chemical Name: 3-Pyridinecarboxylicacid,trimethylsilylester(9CI)
• CAS No.: 25436-37-7
• Molecular Formula: C9H13NO2Si
• Molecular Weight: 195.29100
• Hs Code.: 2933399090
• Mol file: 25436-37-7.mol

Synonyms:trimethylsilyl 3-pyridinecarboxylate;Nicotinic acid-TMS;3-PYRIDINECARBOXYLIC ACID TRIMETHYLSILYL ESTER;

Chemical Property of 3-Pyridinecarboxylicacid,trimethylsilylester(9CI)

Chemical Property:

• PSA: 39.19000
• LogP: 2.07330

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Pyridinecarboxylicacid,trimethylsilylester(9CI)

There total 3 articles about 3-Pyridinecarboxylicacid,trimethylsilylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

nicotinic acid (59-67-6) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → trimethylsilyl 3-pyridinecarboxylate (25436-37-7)

Guidance literature:

With ammonium bisulphate; for 24h; Reflux; Inert atmosphere;

Reference yield: 97.0%

nicotinic acid (59-67-6) + 1,1,1,2,2,2-hexamethyldisilane (1450-14-2) → trimethylsilyl 3-pyridinecarboxylate (25436-37-7)

Guidance literature:

RT, then warmed slowly until violent gas evolution occured;

DOI:10.1016/S0040-4020(01)85961-5

Reference yield:

nicotinic acid (59-67-6) + chloro-trimethyl-silane (75-77-4) → trimethylsilyl 3-pyridinecarboxylate (25436-37-7)

Guidance literature:

With 1,1,1,3,3,3-hexamethyl-disilazane; at 120 ℃; for 5h;

DOI:10.1016/j.bmcl.2004.06.093

upstream raw materials:

nicotinic acid

1,1,1,2,2,2-hexamethyldisilane

chloro-trimethyl-silane

1,1,1,3,3,3-hexamethyl-disilazane

Downstream raw materials:

1-((2R,3R,4S,5R)-3,4-dihydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)pyridin-1-ium-3-carboxylate

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