5-chloro-2-methyl-1H-isoindole-1,3(2H)-dione

Base Information

Chemical Name:5-chloro-2-methyl-1H-isoindole-1,3(2H)-dione
CAS No.:63197-17-1
Molecular Formula:C9H6 Cl N O2
Molecular Weight:195.605
Hs Code.:

Synonyms:Phthalimide,4-chloro-N-methyl- (7CI); 4-Chloro-N-methylphthalimide;N-Methyl-4-chlorophthalimide; NSC 58662

Suppliers and Price of 5-chloro-2-methyl-1H-isoindole-1,3(2H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 5-chloro-2-methyl-1H-isoindole-1,3(2H)-dione

Chemical Property:

Vapor Pressure:0.000435mmHg at 25°C
Boiling Point:315.5°C at 760 mmHg
Flash Point:144.6°C
Density:1.454g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-chloro-2-methyl-1H-isoindole-1,3(2H)-dione

There total 12 articles about 5-chloro-2-methyl-1H-isoindole-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 14737-08-7
4-chloro-1,2,3,6-tetrahydrophthalic anhydride

: 74-89-5
methylamine

: 63197-17-1
N-methyl-4-chlorophthalimide

Guidance literature:: at 150 - 180 ℃; for 3.5h; Neat (no solvent);

Reference yield: 95.0%

: 4-chlorotetrahydrophthalic anhydride

: 63197-17-1
N-methyl-4-chlorophthalimide

Guidance literature:

Reference yield: 74.0%

: 7147-90-2
4-chlorophthalimide

: 74-88-4
methyl iodide

: 63197-17-1
N-methyl-4-chlorophthalimide

Guidance literature:: 4-chlorophthalimide; methyl iodide; With sodium t-butanolate; In toluene; for 0.5h; Reflux;

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 3h; Reflux;