Silanamine, 1,1,1-trimethyl-N,N-diphenyl-

Base Information

• Chemical Name: Silanamine, 1,1,1-trimethyl-N,N-diphenyl-
• CAS No.: 17425-91-1
• Molecular Formula: C15H19 N Si
• Molecular Weight: 241.408
• Hs Code.: 2931900090
• Mol file: 17425-91-1.mol

Synonyms:Silylamine,1,1,1-trimethyl-N,N-diphenyl- (7CI,8CI); (Diphenylamino)trimethylsilane;N-(Trimethylsilyl)diphenylamine

Chemical Property of Silanamine, 1,1,1-trimethyl-N,N-diphenyl-

Chemical Property:

• Vapor Pressure: 0.00126mmHg at 25°C
• Boiling Point: 298.5°Cat760mmHg
• Flash Point: 134.3°C
• PSA: 3.24000
• Density: 0.994g/cm³
• LogP: 4.65960

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Silanamine, 1,1,1-trimethyl-N,N-diphenyl-

There total 7 articles about Silanamine, 1,1,1-trimethyl-N,N-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

chloro-trimethyl-silane (75-77-4) + diphenylamine (122-39-4) → N-(trimethylsilyl)-diphenylamine (17425-91-1)

Guidance literature:

diphenylamine; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at 20 ℃; for 18h;

DOI:10.1039/b509345g

Reference yield: 81.0%

chloro-trimethyl-silane (75-77-4) + lithium diphenylamide (5856-89-3) → N-(trimethylsilyl)-diphenylamine (17425-91-1)

Guidance literature:

In tetrahydrofuran; Ambient temperature;

DOI:10.1016/0022-328X(91)86161-I

Reference yield: 70.0%

trimethyl(pentafluorophenyl)silane (1206-46-8) + diphenylamine (122-39-4) → N-(trimethylsilyl)-diphenylamine (17425-91-1)

Guidance literature:

With (K-18-crown-6 ether) cyanide; In tetrahydrofuran; for 2h;

DOI:10.1007/BF00956809

upstream raw materials:

chloro-trimethyl-silane

lithium diphenylamide

trimethylsilyl trichloroacetate

diphenylamine

Downstream raw materials:

Diphenylaminotetrafluorophosphoran

Hexamethyldisiloxane

tetra-N-phenyl-methylenediamine

(N,N-diphenylcarbamoyl) formyl chloride