1,2-Bis(methylthio)ethane

Base Information

Chemical Name:1,2-Bis(methylthio)ethane
CAS No.:6628-18-8
Molecular Formula:C4H10S2
Molecular Weight:122.255
Hs Code.:2930909090
European Community (EC) Number:801-653-1
NSC Number:60544
UNII:D37463NMIR
DSSTox Substance ID:DTXSID9064427
Nikkaji Number:J101.104I
Wikidata:Q27276036
Metabolomics Workbench ID:45050
Mol file:6628-18-8.mol

Synonyms:2,5-Dithiahexane;1,2-Bis(methylthio)ethane;6628-18-8;1,2-Bis(methylsulfanyl)ethane;1,2-BIS(METHYLMERCAPTO)ETHANE;Ethane, 1,2-bis(methylthio)-;CH3SCH2CH2SCH3;UNII-D37463NMIR;1,2-Bis(methylthio)-Ethane;D37463NMIR;NSC 60544;NSC-60544;Ethane, 1,2-bis(methylthio)- (9CI);NSC60544;Ethane,2-bis(methylthio)-;BIS(METHYLTHIO)ETHANE;1,2-bis(methylsulanyl)ethane;SCHEMBL862384;DTXSID9064427;FEMA NO. 4298;1,2-Bis(methylsulfanyl)ethane #;CHEBI:179052;1,2-Bis(methylthio)ethane, 9CI;2,5-DITHIAHEXANE [FHFI];Q27276036

Suppliers and Price of 1,2-Bis(methylthio)ethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 1,2-Bis(methylthio)ethane

Chemical Property:

Vapor Pressure:1.43mmHg at 25°C
Melting Point:-101.52°C (estimate)
Refractive Index:1.5290
Boiling Point:177°Cat760mmHg
Flash Point:59.9°C
PSA：50.60000
Density:0.997g/cm³
LogP:1.71240
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:122.02239267
Heavy Atom Count:6
Complexity:17.5

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSCCSC

Technology Process of 1,2-Bis(methylthio)ethane

There total 5 articles about 1,2-Bis(methylthio)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 12107-04-9
dicarbonyl(cyclopentadienyl)iron(II) chloride

: 10543-35-8
lithium methylsulfinyl carbanion

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 74-93-1
methylthiol

: 624-92-0
Dimethyldisulphide

: 6628-18-8
1,2-bis(methylthio)ethane

: lithium chloride

Guidance literature:: In tetrahydrofuran; mixing reactants in THF at -78°C, slow warming to room temp.; evapn. in vac., extn. with pentane, ether and finally acetone or CH2Cl2, concn., chromy. on Al2O3, purifn. by crystn., distn. or sublimation;
DOI:10.1016/S0022-328X(00)86902-8

Reference yield: 9.4%

: 88686-82-2
2-Hexyl-1,3,2-dithiaborolane

: 70775-39-2,5367-24-8
dimethylsulfoxonium methylide

: 22322-43-6
2-methylsulfanyl-ethanethiol

: 6628-18-8
1,2-bis(methylthio)ethane

: 7325-10-2
n-hexylboroxine

: 111-27-3
hexan-1-ol

Guidance literature:: With trimethylamine-N-oxide dihydrate; In toluene; treated with 1 equiv. of ylide (0-24°C, 30 min); oxidized with trimethylamine-N-oxide dihydrate (3 equiv.) (60°C, 2 h); GCMS;
DOI:10.1039/b311292f