Technology Process of 1H-Isoindole-5-carboxylic acid, 2,3-dihydro-1-oxo-, methyl ester
There total 6 articles about 1H-Isoindole-5-carboxylic acid, 2,3-dihydro-1-oxo-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
In
methanol;
for 6h;
under 2327.23 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 4 h / 20 - 60 °C / Irradiation
2: ammonium hydroxide; ammonia / methanol / 20 °C
3: triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 140 °C / 22502.3 Torr
With
ammonium hydroxide; N-Bromosuccinimide; ammonia; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; dibenzoyl peroxide;
In
methanol; tetrachloromethane;
- Guidance literature:
-
With
triethylamine;
palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
at 23 - 70 ℃;
Inert atmosphere;