1-(2,3,5,6-Tetrachloro-4-trimethylsilylphenyl)ethanone

Base Information

• Chemical Name: 1-(2,3,5,6-Tetrachloro-4-trimethylsilylphenyl)ethanone
• CAS No.: 86628-51-5
• Molecular Formula: C₁₁H₁₂Cl₄OSi
• Molecular Weight: 330.113
• European Community (EC) Number: 660-682-6
• DSSTox Substance ID: DTXSID70400230
• Wikidata: Q82203098
• Mol file: 86628-51-5.mol

Synonyms:1-(2,3,5,6-tetrachloro-4-trimethylsilylphenyl)ethanone;86628-51-5;2',3',5',6'-TETRACHLORO-4'-(TRIMETHYLSILYL)ACETOPHENONE;DTXSID70400230;AKOS024338733;1-acetyl-4-(trimethylsilyl)tetrachlorobenzene

Chemical Property of 1-(2,3,5,6-Tetrachloro-4-trimethylsilylphenyl)ethanone

Chemical Property:

• Boiling Point: 332.3±42.0 °C(Predicted)
• PSA: 17.07000
• Density: 1.32±0.1 g/cm3(Predicted)
• LogP: 5.04800
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 329.938202
• Heavy Atom Count: 17
• Complexity: 288

Purity/Quality:

2',3',5',6'-TETRACHLORO-4'-(TRIMETHYLSILYL)ACETOPHENONE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)C1=C(C(=C(C(=C1Cl)Cl)[Si](C)(C)C)Cl)Cl

Technology Process of 1-(2,3,5,6-Tetrachloro-4-trimethylsilylphenyl)ethanone

There total 2 articles about 1-(2,3,5,6-Tetrachloro-4-trimethylsilylphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(Trimethylsilyl)-2,3,5,6-tetrachlorobenzene (18713-20-7) + acetyl chloride (75-36-5) → 1-Acetyl-4-(trimethylsilyl)tetrachlorobenzene (86628-51-5)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1007/BF00798443

Reference yield:

chloro-trimethyl-silane (75-77-4) + pentachlorobenzene (608-93-5) + acetyl chloride (75-36-5) → 1,4-Bis(trimethylsilyl)tetrachlorobenzene (15127-70-5) + 1-(Trimethylsilyl)-2,3,5,6-tetrachlorobenzene (18713-20-7) + 1-Acetyl-2,3,5,6-tetrachlorobenzene (86628-50-4) + 1-Acetyl-4-(trimethylsilyl)tetrachlorobenzene (86628-51-5)

Guidance literature:

Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;

DOI:10.1007/BF00798443

upstream raw materials:

chloro-trimethyl-silane

pentachlorobenzene

acetyl chloride

1-(Trimethylsilyl)-2,3,5,6-tetrachlorobenzene