(2,3,5,6-Tetrachlorophenyl)trimethylsilane

Base Information

• Chemical Name: (2,3,5,6-Tetrachlorophenyl)trimethylsilane
• CAS No.: 18713-20-7
• Molecular Formula: C₉H₁₀Cl₄Si
• Molecular Weight: 288.076
• European Community (EC) Number: 660-720-1

Synonyms:(2,3,5,6-TETRACHLOROPHENYL)TRIMETHYLSILANE;AKOS024338700;1-(trimethylsilyl)-2,3,5,6-tetrachlorobenzene

Chemical Property of (2,3,5,6-Tetrachlorophenyl)trimethylsilane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 287.927638
• Heavy Atom Count: 14
• Complexity: 190

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C[Si](C)(C)C1=C(C(=CC(=C1Cl)Cl)Cl)Cl

Technology Process of (2,3,5,6-Tetrachlorophenyl)trimethylsilane

There total 2 articles about (2,3,5,6-Tetrachlorophenyl)trimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-trimethyl-silane (75-77-4) + pentachlorobenzene (608-93-5) + acetyl chloride (75-36-5) → 1,4-Bis(trimethylsilyl)tetrachlorobenzene (15127-70-5) + 1-(Trimethylsilyl)-2,3,5,6-tetrachlorobenzene (18713-20-7) + 1-Acetyl-2,3,5,6-tetrachlorobenzene (86628-50-4) + 1-Acetyl-4-(trimethylsilyl)tetrachlorobenzene (86628-51-5)

Guidance literature:

Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;

DOI:10.1007/BF00798443

Reference yield:

chloro-trimethyl-silane (75-77-4) + 1,2,4,5-tetrachlorobenzene (95-94-3) → 1-(Trimethylsilyl)-2,3,5,6-tetrachlorobenzene (18713-20-7)

Guidance literature:

Multistep reaction; (i) nBuLi, THF, (ii) /BRN= 1209232/;

DOI:10.1016/0022-328X(68)80072-5

Reference yield:

1-(Trimethylsilyl)-2,3,5,6-tetrachlorobenzene (18713-20-7) + acetyl chloride (75-36-5) → 1-Acetyl-4-(trimethylsilyl)tetrachlorobenzene (86628-51-5)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1007/BF00798443

upstream raw materials:

chloro-trimethyl-silane

1,2,4,5-tetrachlorobenzene

pentachlorobenzene

acetyl chloride

Downstream raw materials:

1-Acetyl-4-(trimethylsilyl)tetrachlorobenzene

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