Phenyl 2-methyl-4-oxo-2,3-dihydropyridine-1-carboxylate

Base Information

Chemical Name:Phenyl 2-methyl-4-oxo-2,3-dihydropyridine-1-carboxylate
CAS No.:107971-38-0
Molecular Formula:C13H13NO3
Molecular Weight:231.251
Hs Code.:2933399090
DSSTox Substance ID:DTXSID80426002
Nikkaji Number:J978.065C
Mol file:107971-38-0.mol

Synonyms:107971-38-0;Phenyl 2-methyl-4-oxo-2,3-dihydropyridine-1-carboxylate;PHENYL 3,4-DIHYDRO-2-METHYL-4-OXOPYRIDINE-1(2H)-CARBOXYLATE;SCHEMBL4756495;DTXSID80426002;2-methyl-4-oxo-3,4-dihydro-2h-pyridine-1-carboxylic acid phenyl ester;AB11866;phenyl 2-methyl-4-oxo-3,4-dihydro-1(2H)-pyridinecarboxylate;2-Methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylic acid phenyl ester

Suppliers and Price of Phenyl 2-methyl-4-oxo-2,3-dihydropyridine-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Phenyl 2-methyl-4-oxo-2,3-dihydropyridine-1-carboxylate

Chemical Property:

PSA：46.61000
LogP:2.30030
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:231.08954328
Heavy Atom Count:17
Complexity:332

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CC(=O)C=CN1C(=O)OC2=CC=CC=C2

Technology Process of Phenyl 2-methyl-4-oxo-2,3-dihydropyridine-1-carboxylate

There total 4 articles about Phenyl 2-methyl-4-oxo-2,3-dihydropyridine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 620-08-6,1232006-56-2
4-methoxypyridine

: 676-58-4
methylmagnesium chloride

: 1885-14-9
phenyl chloroformate

: 107971-38-0
N-(phenoxycarbonyl)-2-methyl-2,3-dihydropyrid-4-one

Guidance literature:: In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)82435-1

Reference yield: 74.0%

: 917-64-6
methyl magnesium iodide

: 1-((phenoxy)carbonyl)-4-methoxypyridinium chloride

: 107971-38-0
N-(phenoxycarbonyl)-2-methyl-2,3-dihydropyrid-4-one

Guidance literature:: With oxonium;
DOI:10.1016/S0040-4039(98)01195-2

Reference yield:

: 1122-96-9
4-methoxypyridine N-oxide

: 107971-38-0
N-(phenoxycarbonyl)-2-methyl-2,3-dihydropyrid-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5percent Pd/C / ethanol

2: 1.) THF, -23 deg C, 20 min 2.) 10percent HCl, room temperature, 10 min

With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4039(00)85000-5