N-(Triphenylphosphoranylidene)-4-methoxyaniline

Base Information

Chemical Name:N-(Triphenylphosphoranylidene)-4-methoxyaniline
CAS No.:14796-89-5
Molecular Formula:C25H22NOP
Molecular Weight:383.43
Hs Code.:2931900090
Mol file:14796-89-5.mol

Synonyms:N-(4-Methoxyphenyl)-P,P,P-triphenylphosphine imide;N-(p-Methoxyphenyl)triphenylphosphine imide;N-(Triphenylphosphoranylidene)-4-methoxyaniline

Suppliers and Price of N-(Triphenylphosphoranylidene)-4-methoxyaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of N-(Triphenylphosphoranylidene)-4-methoxyaniline

Chemical Property:

Melting Point:117-118 °C
Boiling Point:541.8±52.0 °C(Predicted)
PSA：31.40000
Density:1.09±0.1 g/cm3(Predicted)
LogP:5.50440

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(Triphenylphosphoranylidene)-4-methoxyaniline

There total 9 articles about N-(Triphenylphosphoranylidene)-4-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2101-87-3
p-methoxy-phenylazide

: 603-35-0
triphenylphosphine

: 14796-89-5
4-methoxy-N-(triphenylphosphoran-ylidene)-aniline

Guidance literature:: In toluene; at 60 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201601125

Reference yield:

: 2101-87-3
p-methoxy-phenylazide

: 603-35-0
triphenylphosphine

: 14796-89-5
4-methoxy-N-(triphenylphosphoran-ylidene)-aniline

: 104-94-9
4-methoxy-aniline

Guidance literature:: In tetrahydrofuran; water; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c8cc00179k

Reference yield:

: 104-94-9
4-methoxy-aniline

: 603-35-0
triphenylphosphine

: 14796-89-5
4-methoxy-N-(triphenylphosphoran-ylidene)-aniline

Guidance literature:: triphenylphosphine; With bromine; In benzene; at -5 - 20 ℃; for 1.33333h; Inert atmosphere;

4-methoxy-aniline; With triethylamine; In benzene; Inert atmosphere; Reflux;
DOI:10.1002/adsc.201000469