Triethyl(silane-d)

Base Information

• Chemical Name: Triethyl(silane-d)
• CAS No.: 1631-33-0
• Molecular Formula: C6H15DSi
• Molecular Weight: 117.271
• European Community (EC) Number: 693-210-2
• DSSTox Substance ID: DTXSID30450711
• Nikkaji Number: J1.615.064I
• Wikidata: Q76416386
• Mol file: 1631-33-0.mol

Synonyms:Triethyl(silane-d);1631-33-0;deuterio(triethyl)silane;Triethylsilane-d1;TRIETHYLSILANE-D 97 ATOM % D;triethyl(?H)silane;Et3SiD;Deuterated triethylsilane;DTXSID30450711;Triethyl(silane-d), 97 atom % D;AKOS015915627;A936891;J-010008

Chemical Property of Triethyl(silane-d)

Chemical Property:

• Refractive Index: n20/D 1.4117(lit.)
• Boiling Point: 107 °C(lit.)
• Flash Point: 25 °F
• PSA: 0.00000
• Density: 0.737 g/mL at 25 °C(lit.)
• LogP: 2.27320
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 117.108403791
• Heavy Atom Count: 7
• Complexity: 25.7

Purity/Quality:

98%Min ^*data from raw suppliers

Triethylsilane-d1 ^*data from reagent suppliers

Safty Information:

• Pictogram(s): F,Xn
• Hazard Codes: F,Xn
• Statements: 11-20/21/22-36/38
• Safety Statements: 16-26-36/37/39-51

MSDS Files:

Useful:

• Canonical SMILES: CC[SiH](CC)CC
• Isomeric SMILES: [2H][Si](CC)(CC)CC

Technology Process of Triethyl(silane-d)

There total 1 articles about Triethyl(silane-d) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylsilyl chloride (994-30-9) + benzene-d6 (1076-43-3) → Et3SiD (1631-33-0) + C12H15(2)H5Si (95450-76-3)

Guidance literature:

With calcium; Yield given. Multistep reaction. Yields of byproduct given; 1) 900 deg C, 0.005 Torr, 2) 1 h, r.t., 0.005 Torr;

DOI:10.1246/cl.1984.1989

Reference yield: 100.0%

Et3SiD (1631-33-0) + benzaldehyde (100-52-7) → hexaethyl disiloxane (994-49-0) + C14H12(2)H2O

Guidance literature:

With uranyl(VI) triflate; In dichloromethane-d2; at 20 ℃; for 1h;

DOI:10.1021/acscatal.9b01408

Reference yield: 85.0%

Et3SiD (1631-33-0) + 2-Benzyloxymethyl-3-(2-trimethylsilanyl-1-triphenylsilanyloxy-allyl)-oxirane (130659-94-8) → C34H39(2)HO3Si2 (130659-98-2)

Guidance literature:

With titanium tetrachloride; In dichloromethane; at -78 ℃;

DOI:10.1016/S0040-4039(00)89058-9

upstream raw materials:

triethylsilyl chloride

benzene-d6

Downstream raw materials:

α,β-dideuterio-β-(triethylsilyl)styrene

C₁₆H₂₅⁽²⁾HO₃Si

C₃₄H₃₉⁽²⁾HO₃Si₂

triethylsilyl fluoride

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