N',N'-Dibenzylbenzohydrazide

Base Information

Chemical Name:N',N'-Dibenzylbenzohydrazide
CAS No.:6304-45-6
Molecular Formula:C21H20 N2 O
Molecular Weight:316.403
Hs Code.:2928000090
NSC Number:42957
DSSTox Substance ID:DTXSID30212331
Nikkaji Number:J2.481.216B
Wikidata:Q83087416
ChEMBL ID:CHEMBL1881695
Mol file:6304-45-6.mol

Synonyms:DBBHD;N',N'-dibenzylbenzohydrazide

Suppliers and Price of N',N'-Dibenzylbenzohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of N',N'-Dibenzylbenzohydrazide

Chemical Property:

Melting Point:166 °C
PKA:12.52±0.46(Predicted)
PSA：32.34000
Density:1.150±0.06 g/cm3(Predicted)
LogP:4.42470
XLogP3:4.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:316.157563266
Heavy Atom Count:24
Complexity:346

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CN(CC2=CC=CC=C2)NC(=O)C3=CC=CC=C3

Technology Process of N',N'-Dibenzylbenzohydrazide

There total 8 articles about N',N'-Dibenzylbenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 98-88-4
benzoyl chloride

: 5802-60-8
N,N-dibenzylhydrazine

: 6304-45-6
N′,N′-dibenzylbenzohydrazide

Guidance literature:: With sodium hydrogencarbonate;
DOI:10.1021/jf0704211

Reference yield: 85.0%

: 613-94-5
benzoic acid hydrazide

: 100-51-6,185532-71-2
benzyl alcohol

: 6304-45-6
N′,N′-dibenzylbenzohydrazide

Guidance literature:: With t-butylnitrite; (1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one)ruthenium tricarbonyl complex; sodium t-butanolate; In tert-butyl alcohol; at 130 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.1c00654

Reference yield: 78.0%

: 100-52-7
benzaldehyde

: 613-94-5
benzoic acid hydrazide

: 1215-52-7
N-benzoyl-N'-benzylhydrazine

: 6304-45-6
N′,N′-dibenzylbenzohydrazide

Guidance literature:: benzaldehyde; benzoic acid hydrazide; With borane pyridine; acetic acid; In methanol; at 0 - 20 ℃; for 2h;

With hydrogenchloride; In methanol; water; at 0 - 20 ℃; for 0.5h;
DOI:10.1055/s-0033-1340484