N'-Propionylpropionohydrazide

Base Information

• Chemical Name: N'-Propionylpropionohydrazide
• CAS No.: 1528-34-3
• Molecular Formula: C6H12 N2 O2
• Molecular Weight: 144.173
• Hs Code.: 2928000090
• European Community (EC) Number: 216-205-5
• DSSTox Substance ID: DTXSID70934601
• Nikkaji Number: J206.739K
• Wikidata: Q82910506
• Mol file: 1528-34-3.mol

Synonyms:N'-Propionylpropionohydrazide;1528-34-3;N'-propanoylpropanehydrazide;2'-(1-Oxopropyl)propionohydrazide;1,2-Dipropionylhydrazine;EINECS 216-205-5;2/'-(1-oxopropyl)propionohydrazide;dipropionyl hydrazine;N,N'-Dipropionylhydrazine;N/'-Propanoylpropanehydrazide;SCHEMBL1169137;DTXSID70934601;AKOS024340001;SB86624;Propanoic acid, 2-(1-oxopropyl)hydrazide;N-(1-Hydroxypropylidene)propanehydrazonic acid;A883871

Chemical Property of N'-Propionylpropionohydrazide

Chemical Property:

• Boiling Point: 350.1°Cat760mmHg
• Flash Point: 168°C
• PSA: 65.18000
• Density: 1.033g/cm³
• LogP: 1.63440
• XLogP3: 0
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 144.089877630
• Heavy Atom Count: 10
• Complexity: 118

Purity/Quality:

99% ^*data from raw suppliers

1,2-DIPROPIONYLHYDRAZINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC(=O)NNC(=O)CC

Technology Process of N'-Propionylpropionohydrazide

There total 7 articles about N'-Propionylpropionohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

propionyl chloride (79-03-8) + d'hydrazide de l'acide propionique (5818-15-5) → N1,N2-dipropionylhydrazine (1528-34-3)

Guidance literature:

With potassium carbonate; In water; at 0 - 20 ℃; for 3.5h;

DOI:10.1039/c7nj00965h

Reference yield:

Ethyl propionate (105-37-3,20741-13-3) → N1,N2-dipropionylhydrazine (1528-34-3) + d'hydrazide de l'acide propionique (5818-15-5)

Guidance literature:

With hydrazine hydrate;

Reference yield:

propionic acid anhydride (123-62-6) → N1,N2-dipropionylhydrazine (1528-34-3)

Guidance literature:

With hydrazine hydrate;

DOI:10.1021/jo50009a006

upstream raw materials:

methanol

dipropionyl-diazene

d'hydrazide de l'acide propionique

Ethyl propionate

Downstream raw materials:

1,2-di-n-propylhydrazine

3,4-hexanedione

5-ethyl-1-(3-nitro-phenyl)-1H-tetrazole

2,5-diethyl-1,3,4-oxadiazole

Refernces

• 1、 Drozdetskii,Radushev,Turbin,Gusev,Drozdova,Shekhonina,Chekanova. "Parameters of synthesis of hydrazides and 1,2-diacylhydrazines by thermal decomposition of hydrazine salts of aliphatic carboxylic acids". . p. 302 - 306. Retrieved 2007/10/03.