3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline

Base Information

Chemical Name:3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline
CAS No.:1311401-73-6
Molecular Formula:C₁₈H₁₈F₃IN₂O₅
Molecular Weight:526.251
Hs Code.:

Synonyms:3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline

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Chemical Property of 3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline

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Technology Process of 3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline

There total 4 articles about 3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.3%

: 765962-71-8
(2-fluoro-4-iodo-phenyl)-(2,3,5-trifluoro-6-nitro-phenyl)-amine

: 621-63-6
glycoaldehyde diethyl acetal

: 1311401-73-6
3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline

Guidance literature:: glycoaldehyde diethyl acetal; With sodium hydride; In tetrahydrofuran; at 0 - 5 ℃; for 2h; Industry scale;

(2-fluoro-4-iodo-phenyl)-(2,3,5-trifluoro-6-nitro-phenyl)-amine; In tetrahydrofuran; at 0 - 20 ℃; for 65h; Product distribution / selectivity; Industry scale;

Reference yield:

: 29632-74-4
2-fluro-4-iodoaniline

: 1311401-73-6
3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 1 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0 - 40 °C

2.2: 0 - 20 °C

With sodium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; hexane;

Reference yield:

: 314-41-0
1,2,3,5-tetrafluoro-4-nitrobenzene

: 1311401-73-6
3-(2,2-diethoxyethoxy)-5,6-difluoro-N-(2-fluoro-4-iodophenyl)-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 1 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0 - 40 °C

2.2: 0 - 20 °C

With sodium hydride; lithium hexamethyldisilazane; In tetrahydrofuran; hexane;