1-Butanamine, N-(2-methylpropyl)-

Base Information

• Chemical Name: 1-Butanamine, N-(2-methylpropyl)-
• CAS No.: 20810-06-4
• Molecular Formula: C8H19N
• Molecular Weight: 129.246
• Hs Code.: 2921199090
• European Community (EC) Number: 244-051-9
• UNII: 66MVU4W883
• DSSTox Substance ID: DTXSID6066654
• Nikkaji Number: J43.292J
• Wikidata: Q27264009
• Mol file: 20810-06-4.mol

Synonyms:1-Butanamine, N-(2-methylpropyl)-;20810-06-4;N-Isobutylbutylamine;N-(2-methylpropyl)butan-1-amine;butyl isobutyl amine;66MVU4W883;Butylisobutyl amine;butyl(2-methylpropyl)amine;isobutyl-n-butyl-amine;N-Butyl-2-methylpropylamine;SCHEMBL271458;UNII-66MVU4W883;DTXSID6066654;N-(2-methylpropyl)-1-butanamine;EINECS 244-051-9;AKOS000234681;N-BUTYL-2-METHYL-PROPAN-1-AMINE;Q27264009

Chemical Property of 1-Butanamine, N-(2-methylpropyl)-

Chemical Property:

• Vapor Pressure: 3.34mmHg at 25°C
• Boiling Point: 153.4°Cat760mmHg
• Flash Point: 31.8°C
• PSA: 12.03000
• Density: 0.761g/cm³
• LogP: 2.42300
• XLogP3: 2.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 129.151749610
• Heavy Atom Count: 9
• Complexity: 50.5

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCCCNCC(C)C

Technology Process of 1-Butanamine, N-(2-methylpropyl)-

There total 10 articles about 1-Butanamine, N-(2-methylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

1-bromo-butane (109-65-9) + isobutylamine (78-81-9) → n-butylisobutylamine (20810-06-4)

Guidance literature:

for 7h; Reflux;

DOI:10.1021/jo802016t

Reference yield: 53.0%

propyl cyanide (109-74-0) + 2-methyl-propan-1-ol (78-83-1) → n-butylisobutylamine (20810-06-4) + dibutylamine (111-92-2)

Guidance literature:

With Co(9.8%)/SiO2 catalyst; hydrogen; at 129.84 ℃; under 9750.98 Torr;

DOI:10.1016/j.jcat.2019.10.011

Reference yield:

N-Butyl-2-methylpropanamide (6282-85-5) → n-butylisobutylamine (20810-06-4)

Guidance literature:

With hydrogen; In 1,2-dimethoxyethane; at 160 ℃; for 20h; under 22502.3 Torr; Inert atmosphere; Autoclave; Molecular sieve;

DOI:10.1002/anie.201207803

upstream raw materials:

butyl-isobutyl-carbamonitrile

N-butylamine

isobutyraldehyde

1-bromo-butane

Downstream raw materials:

Cyclohexen-1-yl-n-butylisobutylamin

Refernces

• 1、 Stein, Mario,Breit, Bernhard. "Catalytic hydrogenation of amides to amines under mild conditions". supporting information. p. 2231 - 2234. Retrieved 2013/03/28.