5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione

Base Information

Chemical Name:5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione
CAS No.:114751-23-4
Molecular Formula:C₁₄H₂₀O₃
Molecular Weight:236.311
Hs Code.:

Synonyms:5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione

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Chemical Property of 5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione

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Technology Process of 5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione

There total 4 articles about 5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 61565-12-6
2,2,4,4-tetramethyl-6-(2-methylpropylidene)-cyclohexane-1,3,5-trione

: 114751-23-4
5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione

Guidance literature:: In benzene; for 1h; Heating;
DOI:10.1016/S0031-9422(00)82514-5

Reference yield:

: 77744-52-6
5-hydroxy-2,2,6,6-tetramethyl-cyclohex-4-ene-1,3-dione

: 78-84-2
isobutyraldehyde

: 114751-23-4
5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione

Guidance literature:: 5-hydroxy-2,2,6,6-tetramethyl-cyclohex-4-ene-1,3-dione; isobutyraldehyde; With piperidine; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

With hydrogenchloride; ammonium chloride; In dichloromethane; water; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2022.132631

Reference yield:

: 77744-52-6
5-hydroxy-2,2,6,6-tetramethyl-cyclohex-4-ene-1,3-dione

: 114751-23-4
5-hydroxy-2,2,6,6-tetramethyl-4-(2-methylprop-1-en-yl)cyclohex-4-ene-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 3.05 g / diethyl ether / 0.08 h / Ambient temperature

2: 86 percent / p-TsOH / CH₂Cl₂ / 0.17 h / Ambient temperature

3: 100 percent / benzene / 1 h / Heating

With toluene-4-sulfonic acid; In diethyl ether; dichloromethane; benzene;
DOI:10.1016/S0031-9422(00)82514-5