2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione

Base Information

Chemical Name:2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione
CAS No.:114751-25-6
Molecular Formula:C₁₈H₂₉NO₃
Molecular Weight:307.433
Hs Code.:

Synonyms:2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione

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Chemical Property of 2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione

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Technology Process of 2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione

There total 1 articles about 2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-75-1
pyrrolidine

: 77744-52-6
5-hydroxy-2,2,6,6-tetramethyl-cyclohex-4-ene-1,3-dione

: 78-84-2
isobutyraldehyde

: 114751-25-6
2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione

Guidance literature:: In diethyl ether; for 0.0833333h; Ambient temperature;
DOI:10.1016/S0031-9422(00)82514-5

Reference yield: 86.0%

: 114751-25-6
2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione

: 61565-12-6
2,2,4,4-tetramethyl-6-(2-methylpropylidene)-cyclohexane-1,3,5-trione

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; for 0.166667h; Ambient temperature;
DOI:10.1016/S0031-9422(00)82514-5

Reference yield:

: 114751-25-6
2,2,4,4-Tetramethyl-6-(2-methyl-1-pyrrolidin-1-yl-propyl)-cyclohexane-1,3,5-trione

: 5-Methoxy-2,2,6,6-tetramethyl-4-(2-methyl-propenyl)-cyclohex-4-ene-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / p-TsOH / CH₂Cl₂ / 0.17 h / Ambient temperature

2: 100 percent / benzene / 1 h / Heating

3: 1 g / diethyl ether / 0.5 h / 0 °C

With toluene-4-sulfonic acid; In diethyl ether; dichloromethane; benzene;
DOI:10.1016/S0031-9422(00)82514-5