[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF₂

Base Information

• Chemical Name: [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF₂
• CAS No.: 1166392-55-7
• Molecular Formula: C₃₆H₃₀BF₂N₃O₄
• Molecular Weight: 617.46
• Mol file: 1166392-55-7.mol

Synonyms:[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF₂

Chemical Property of [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF₂

There total 5 articles about [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine (873975-75-8) + boron trifluoride diethyl etherate (109-63-7) → [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF2 (1166392-55-7)

Guidance literature:

[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.166667h;

boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1007/s10895-020-02646-4

Reference yield:

4,4'-dimethoxychalcone (2373-89-9) → [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF2 (1166392-55-7)

Guidance literature:

Multi-step reaction with 2 steps

1: diethylamine / methanol / Reflux

2: triethylamine / methanol / Reflux

With diethylamine; triethylamine; In methanol;

DOI:10.1021/acs.orglett.7b01133

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF2 (1166392-55-7)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide / methanol

2: diethylamine / methanol / Reflux

3: triethylamine / methanol / Reflux

With diethylamine; triethylamine; potassium hydroxide; In methanol;

DOI:10.1021/acs.orglett.7b01133

upstream raw materials:

1-(4-methoxyphenyl)ethanone

4-methoxy-benzaldehyde

4,4'-dimethoxychalcone

boron trifluoride diethyl etherate