(4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1⁽²⁰⁾,17-diene-2,5,13,16-tetraone

Base Information

• Chemical Name: (4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1⁽²⁰⁾,17-diene-2,5,13,16-tetraone
• CAS No.: 87831-14-9
• Molecular Formula: C₃₀H₃₉N₃O₈
• Molecular Weight: 569.655

Synonyms:(4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1⁽²⁰⁾,17-diene-2,5,13,16-tetraone

Chemical Property of (4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1⁽²⁰⁾,17-diene-2,5,13,16-tetraone

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Technology Process of (4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1⁽²⁰⁾,17-diene-2,5,13,16-tetraone

There total 1 articles about (4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1⁽²⁰⁾,17-diene-2,5,13,16-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

(4S,14S)-4,14-di-(2-propyl)-19-methyl-6,9,12-trioxa-3,15-diaza-19-azoniabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,5,13,16-tetraone perchlorate + acetophenone (98-86-2) → (4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1(20),17-diene-2,5,13,16-tetraone (87831-14-9) + (4S,14S)-4,14-Diisopropyl-19-methyl-18-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1(20),17(21)-diene-2,5,13,16-tetraone

Guidance literature:

With 2,6-dichloro-benzonitrile; In dimethyl sulfoxide; at 25 ℃;

DOI:10.1021/ja00364a079

Reference yield: 73.0%

benzaldehyde (100-52-7) + (4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1(20),17-diene-2,5,13,16-tetraone (87831-14-9) → 3-hydroxy-1,3-diphenylpropan-1-one (42052-51-7)

Guidance literature:

With magnesium(II) perchlorate; In acetone; at 20 ℃;

DOI:10.1021/ja00364a079

Reference yield: 59.0%

pivalaldehyde (630-19-3) + (4S,14S)-4,14-Diisopropyl-19-methyl-21-(2-oxo-2-phenyl-ethyl)-6,9,12-trioxa-3,15,19-triaza-bicyclo[15.3.1]henicosa-1(20),17-diene-2,5,13,16-tetraone (87831-14-9) → 3-hydroxy-1-phenyl-4,4-dimethyl-pentan-1-one (80926-17-6)

Guidance literature:

With magnesium(II) perchlorate; In acetone; at 20 ℃;

DOI:10.1021/ja00364a079

upstream raw materials:

acetophenone

Downstream raw materials:

3-hydroxy-1,3-diphenylpropan-1-one

3-hydroxy-1-phenyl-4,4-dimethyl-pentan-1-one

3-hydroxy-4-methyl-1-phenylpentan-1-one

3-hydroxy-3-(2-methoxy-phenyl)-1-phenyl-propan-1-one

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