trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate

Base Information

Chemical Name:trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate
CAS No.:10416-74-7
Molecular Formula:C₁₃H₂₆O₃Si₂
Molecular Weight:286.519
Hs Code.:

Synonyms:trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate

Suppliers and Price of trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate

There total 4 articles about trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 6651-36-1
1-(Trimethylsilyloxy)cyclohexene

: 124-38-9,18923-20-1
carbon dioxide

: 74-88-4
methyl iodide

: 28746-99-8
1'-hydroxy-bicyclohexyl-2-one

: 10416-74-7
trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 583-60-8
2-Methylcyclohexanone

Guidance literature:: 1-(Trimethylsilyloxy)cyclohexene; With methyllithium; In diethyl ether; at 0 - 25 ℃; for 1h; Inert atmosphere; Schlenk technique;

carbon dioxide; In diethyl ether; at 25 ℃; for 1.5h; under 750.075 Torr; Inert atmosphere; Schlenk technique;

chloro-trimethyl-silane; methyl iodide; Further stages;
DOI:10.1021/jacs.7b08450

Reference yield:

: 6651-36-1
1-(Trimethylsilyloxy)cyclohexene

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 10416-74-7
trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

Guidance literature:: 1-(Trimethylsilyloxy)cyclohexene; With carbon dioxide; methyllithium; lithium iodide; In tetrahydrofuran-d8; at -78 - 20 ℃; Inert atmosphere; Schlenk technique;

1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran-d8; at 25 ℃; for 1.5h; Inert atmosphere; Schlenk technique;

With chloro-trimethyl-silane; In tetrahydrofuran-d8; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.7b08450

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: lithium 2-oxocyclohexane-1-carboxylate

: 10416-74-7
trimethylsilyl 2-((trimethylsilyl)oxy)cyclohex-1-en-1-carboxylate

: trimethylsilyl 2-oxocyclohexane-1-carboxylate

Guidance literature:: With carbon dioxide; In diethyl ether; at -78 - 20 ℃; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.7b08450