p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside
CAS No.:942044-20-4
Molecular Formula:C₃₈H₃₄O₆S
Molecular Weight:618.75
Hs Code.:

Synonyms:p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside

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Chemical Property of p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside

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Technology Process of p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside

There total 6 articles about p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 942043-54-1
p-methylphenyl 4,6-O-benzylidine-3-O-(naphthalen-2-ylmethyl)-1-thio-β-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 942044-20-4
p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/bc500575a

Reference yield: 78.0%

: 942043-17-6
4-methylphenyl 2,3,4,6-tetrakis-O-trimethylsilyl-1-thio-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 100-52-7
benzaldehyde

: 66-99-9
β-naphthaldehyde

: 93-97-0
benzoic acid anhydride

: 942043-30-3
4-methylphenyl 2-O-benzoyl-4,6-O-benzylidene-3-O-benzyl-1-thio-β-D-glucopyranoside

: 942044-14-6
4-methylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidine1-thio-β-D-galactopyranoside

: 942044-19-1
C₃₃H₃₂O₆S

: 942044-20-4
p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside

Guidance literature:: 4-methylphenyl 2,3,4,6-tetrakis-O-trimethylsilyl-1-thio-β-D-glucopyranoside; benzaldehyde; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 ℃; for 2h; Molecular sieve;

benzaldehyde; β-naphthaldehyde; With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 ℃; for 5h; Combinatorial reaction / High throughput screening (HTS);

acetic anhydride; benzoic acid anhydride; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 - 0 ℃; Product distribution / selectivity; Combinatorial reaction / High throughput screening (HTS);

Reference yield: 75.0%

: 942043-17-6
4-methylphenyl 2,3,4,6-tetrakis-O-trimethylsilyl-1-thio-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 100-52-7
benzaldehyde

: 123-11-5
4-methoxy-benzaldehyde

: 98-88-4
benzoyl chloride

: 66-99-9
β-naphthaldehyde

: 942043-30-3
4-methylphenyl 2-O-benzoyl-4,6-O-benzylidene-3-O-benzyl-1-thio-β-D-glucopyranoside

: 942044-14-6
4-methylphenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidine1-thio-β-D-galactopyranoside

: 942044-15-7
C₃₀H₃₂O₇S

: 942044-19-1
C₃₃H₃₂O₆S

: 942044-16-8
p-methylphenyl 4,6-O-benzylidene-2-O-benzoyl-3-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside

: 942044-20-4
p-tolyl 2-O-benzoyl-4,6-O-benzylidene-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-glucopyranoside

Guidance literature:: 4-methylphenyl 2,3,4,6-tetrakis-O-trimethylsilyl-1-thio-β-D-glucopyranoside; benzaldehyde; β-naphthaldehyde; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 ℃; for 2h; Molecular sieve; Combinatorial reaction / High throughput screening (HTS);

benzaldehyde; 4-methoxy-benzaldehyde; β-naphthaldehyde; With triethylsilane; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -86 ℃; for 5h; Combinatorial reaction / High throughput screening (HTS);

acetic anhydride; benzoyl chloride; With tetrabutyl ammonium fluoride; triethylamine; more than 3 stages; Product distribution / selectivity;